stress-relief, annealing and normalizing

Stress-Relief Heat Treatments

There are many effects and sources of residual stress in steels. Tensile surface residual stresses are detrimental and may cause cracking during fabrication or reduced resistance to fracture in service, whereas surface compressive stresses are generally beneficial and prevent cracking during manufacture and service. Short of cracking, residual stresses may cause distortion and undesired dimensional changes. A major source of residual stresses during heat treatment is expansion or contraction of surface microstructures at different times than interior microstructures because of differences in surface and interior cooling or heating rates. Control of residual stresses during the various stages of hardening is a major consideration in all phases of the heat treatment of tool steels. In tool steels, residual stress-relief treatments are most commonly performed following machining and grinding operations to shape a finished tool. These operations may introduce plastic deformation and high surface strains, typically in annealed, machinable ferrite-carbide microstructures, which on subsequent hardening may cause distortion and cracking. Grinding operations applied to hardened tools with tempered martensitic microstructures, or to tools that have been work hardened in service, may also cause cracking and high residual stresses before or during service .To maintain hardness, stress-relief treatments on reground tool steels should be performed at temperatures at or below the tempering temperatures used to produce the required hardness of the tool.

stress-relief heat treatments are generally of short duration (1 to 2 h) or, in larger sections, 1 h/25 mm (1 in.) of section thickness.

The temperatures for stress-relief heat treatments are typically between 550 and 650 °C (1020 and 1200 °F) for plain carbon and low-alloy steels and between 600 and 750 °C (1110 and 1380 °F) for hot-work and high-speed steels. As noted earlier, stress relief is also a function of time at temperature, but generally temperature has a much stronger effect on the kinetics of stress relief than does time. Heavy sections should be cooled very slowly from stress-relief temperatures.

to at least 300 °C (570 °F) (Ref 4) and then air cooled. Otherwise, distortion and new residual stresses may be introduced due to uneven cooling of surfaces and interiors,

Annealing

Annealing heat treatments are designed to soften tool steel microstructures, primarily for the machining stages of manufacture, but also to provide microstructural uniformity for subsequent hardening heat treatments. The softening demonstrates the great versatility of carbon-base tool steels, which can be sequentially heat treated to produce machinable annealed microstructures with very low hardness followed by hardening to essentially unworkable microstructures of very high hardness. Although many tool steels may not be normalized, almost all tool steels are subjected to annealing.

Very slow rates of furnace cooling from the annealing temperatures, from 8 to 22 °C/h (14 to 40 °F/h) depending on steel composition are also a necessary part of annealing. When a steel cools to 500°C (930 °F), essentially all transformation is completed, and air cooling can be used to bring the steel to room temperature. Controlled-atmosphere furnaces, salt baths, and vacuum furnaces used to protect tool steels from oxidation and decarburization during annealing.

The microstructural objective of annealing is to produce dispersed, spherical carbides in a matrix of ferrite grains, a microstructure that is highly machinable compared to other microstructures formed in tool steels. Ferrite has low strength, and the continuous ferrite matrix easily deforms.

Normalizing

This heat treatment is applied to tool steels that have been forged at high temperatures, as shown in Fig. 5-3. Forging deformation, depending on part geometry, may cause localized variations in microstructure and, because of the high temperatures used, may produce a coarse, austenitic grain structure. Normalizing is performed to produce more uniform, fine-grained microstructures for subsequent annealing and hardening heat treatments. Also, in tool steels with high stable carbide contents, the carbides may be preferentially aligned in the direction of hot work, and normalizing will help to produce more uniform distributions.

The cross-hatched temperature region shown in Fig. 5-3, then air cooling. As shown, the normalizing temperatures for hypereutectoid steels approach and sometimes exceed Acm temperatures. Therefore, during heating to and holding at the normalizing temperature, austenite grains nucleate and grow from the ferrite-carbide microstructures stable at low temperatures. Considerable carbide dissolution, depending on alloy content, takes place during heating. During cooling, austenite then transforms to mixtures of ferrite and cementite. If the alloy content of a tool steel is low, cementite and pearlitic microstructures will form during air cooling, and the carbides in these structures will be spheroidized in subsequent annealing treatments. In hypereutectoid steels, where the microstructure is completely converted to austenite during normalizing, cementite networks will form on austenite grain boundaries on cooling prior to pearlite formation.

In tool steels with high alloy content, high hardenability may cause martensite to form during air cooling. Hardenability is the topic which relates alloying to the phase transformations that occur on cooling . Although air hardening in tool steels with high hardenability is a beneficial characteristic during final hardening, martensite formation combined with the high austenitizing temperatures of normalizing may cause cracking, especially if carbide networks that provide pathways for brittle fracture are present. Therefore, air-hardening tool steels usually are not normalized.

Schematic diagram showing approximate temperature ranges, relative to the Fe-C phase diagram, for various carbon and tool steel heat treatments.

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